《Table 2 Enzymatic and cellular activities(IC50,nmol·L-1)of the analogues of FGF401》

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《通过FGF401的构效关系研究发现一种新颖的FGFR4选择性抑制剂（英文）》

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1H NMR and 13C NMR spectra were recorded on a Bruker Avance ARX-400.Mass spectra were performed on a Kompact Axima-CFR MALDI mass spectrometers.Optical rotations were recorded on a Perkin Elmer 341polarimeter.Anhydrous tetrahydrofuran（THF）were obtained by distillation from sodium.All other solvents werereagent grade that were used without any pretreatment.The progress of all reactions was monitored by thin-layer chromatography（TLC）using ethyl acetate/n-hexane as solvent system，and spots were visualized by irradiation with ultraviolet light（254 nm）or staining with phosphomolybdic acid.Flash chromatography was performed using silica gel（200～300 mesh）.