《Table 1 Crystal structural data and refinement parameters for complex 1》

《Table 1 Crystal structural data and refinement parameters for complex 1》   提示:宽带有限、当前游客访问压缩模式
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《五配位单核钴配合物的单晶结构和磁性能(英文)》


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Single-crystal diffraction data were recorded on a Bruker D8 QUEST diffractometer with Mo Kα(λ=0.071 073 nm)radiation at 120 K.The crystal structure was solved by direct methods,and all non-hydrogen atoms were refined anisotropically by least-squares on F2using the SHELXTL 2014/7 program[6].Hydrogen atoms on organic ligands were generated by the riding mode.The responses to the alerts from checkCIF are quoted within the validation response form.The details of single-crystal diffraction data and selected bond lengths and bond angles are listed in Table 1and 2,respectively.