《Table 1 Crystallographic data and structure refinement details for 4》

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《2-吡唑啉-9-芳基邻菲咯啉镍配合物催化芳基卤化物和格氏试剂偶联反应的研究（英文）》

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Diffraction data for the complexes were collected on a Bruker SMART APEX II diffractometer at room temperature（293 K）with graphite-monochromated Mo Kαradiation（λ=0.710 73）.An empirical absorption correction using SADABS was applied for all data.The structures were solved by direct methods using the SHELXS program.All non-hydrogen atoms were refined anisotropically by full-matrix least-squares on F2by the use of the program SHELXL.The hydrogen atoms bonded to carbon were included in idealized geometric positions with thermal parameters equivalent to1.2 times those of the atom to which they were attached.Crystallographic data for the complexes 4 are listed in Table 1.