《Table 1 Crystal data and structure refinement for complexes 1~3》

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《"2,6-二甲基-3,5-二庚酮稀土配合物的合成、结构以及光学性能研究（英文）"》

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The single-crystal X-ray data of complexes 1~3 were collected using an Oxford Xcalibur Gemini Ultra diffractometer with graphite-monochromated Mo Kα（λ=0.071 073 nm）at room temperature.The empirical absorption corrections based on the equivalent reflections were applied.The structures of complexes 1~3 were characterized by the direct method and refined using the full matrix least-squares method on F2using the SHELXS-97 crystallographic software package[18].All non-hydrogen atoms were anisotropically refined.The crystal data and structure refinement details for complexes 1~3 were summarized in Table 1.The selected bond lengths and angles for complexes 1~3 were given in Table 1.CCDC No.1812286~1812288 contained the supplementary crystallographic data for complexes 1~3，respectively.These data were obtained free of charge from the Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.