《Table 1.Crystal Data and Structure Refinement for Compounds 1～3》

《Table 1.Crystal Data and Structure Refinement for Compounds 1～3》   提示：宽带有限、当前游客访问压缩模式
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《A Series of Lanthanide-organic Frameworks Constructed by Ln_4(OH)_4 Clusters and Mixed Ligands》


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aR=Σ|Fo|–|Fc|/Σ|Fo|，bwR={Σ[w（Fo2–Fc2）2]/Σ[w（Fo2）2]}1/2

The intensity data were collected on a Bruker APEX II（1～3）with graphite-monochromated Mo-Kαradiation（λ=0.71073?）at room temperature.All absorption corrections were performed using the multi-scan program.The structures were solved by direct methods and refined by full-matrix least-squares on F2 with the SHELXS-97 and SHELXL-97 programs[20].The hydrogen atoms of ligands were calculated with the riding model，while the hydrogen atoms of OH groups were located from Fourier difference maps.All atoms except H atoms were refined anisotropically.Further details for structural analyses of 1～3 are summarized in Table 1，and selected bond lengths of them are listed in Table 2.

图表编号XD0034854700    严禁用于非法目的
绘制时间2019.01.01
作者顾翔宇、金聪聪、程建文
绘制单位Key Laboratory of the Ministry of Education for Advanced Catalysis Materials, Institute of Physical Chemistry, Zhejiang Normal University、Key Laboratory of the Ministry of Education for Advanced Catalysis Materials, Institute of Physical Chemistry, Zhejia
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