《表S1 M和BP5在不同当量比的纯水中形成水凝胶SH-BP5的转融温度（Tgel)》

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《基于柱[5]芳烃主客体包结构筑分子响应型超分子水凝胶（英文）》

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All other reagents and solvents were commercially available at analytical grade and were used without further purification.1H NMR spectra and 13C NMR spectra（151 MHz）were recorded on Mercury-400BB spectrometer（400 MHz）and Bruker Digital RF spectrometer（300 MHz）.1H chemical shifts are reported in ppm downfield from tetramethylsilane（TMS，TM scale with the solvent resonances as internal standards）.Mass spectrum was performed on a Bruker Esquire3000 plus mass spectrometer（Bruker-Franzen Analytik Gmb H Bremen，Germany）equipped with ESI interface and ion trap analyzer.The morphologies and sizes of the xerogels were characterized using field emission scanning electron microscopy（FE-SEM，JSM-6701F）at an accelerating voltage of 8 k V.The X-ray diffraction analysis（XRD）was performed in a transmission mode with a Rigaku RINT 2000 diffractometer equipped with graphite monochromated Cu Ka radiation（λ=1.54073?）.Fluorescence spectra were recorded on a Shimadzu RF-5301PC spectrofluorophotometer.