《Table 2 Synthesis of biotin conjugated glaucocalyxin A(BcGLA).Isolated yields are reported》

《Table 2 Synthesis of biotin conjugated glaucocalyxin A(BcGLA).Isolated yields are reported》   提示：宽带有限、当前游客访问压缩模式
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《原位Cu(Ⅰ)催化的叠氮-炔环加成反应合成长链双功能分子：蓝萼甲素与生物素的长链轭合分子的制备（英文）》


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Chemicals，commercially available，were purchased from Engergy Chemical，Innochem，Aladdin，or J&K，and used without any further purification.Analytical thin layer chromatography（TLC）was performed on precoated TLC plates（layer 0.20 mm silica gel 60 with fluorescent indicator(UV 254:Merck）).The semi-preparation liquid chromatography（HS-2900P，5μm C18(2）100?)，and the eluents were MeOH/H2O（V∶V=3∶7～3∶2）.The TLC plates were air-dried and revealed under UV lamp（254/365 nm）.1H NMR and 13C NMR spectra were recorded on a Bruker DPX-400 spectrometer.

图表编号XD009802300    严禁用于非法目的
绘制时间2019.06.01
作者程懂懂、张运晓、王金明、白素平
绘制单位郑州大学化学与分子工程学院、郑州大学化学与分子工程学院、郑州大学化学与分子工程学院、新乡医学院药学院
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