《Table 1 Crystallographic data for complex 1》

《Table 1 Crystallographic data for complex 1》   提示:宽带有限、当前游客访问压缩模式
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《"[Zn(Pybox)Br_2]配合物的合成,晶体结构及催化性质研究(英文)"》


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*R1=Σ||Fo|-|Fc||/Σ|Fo|;wR2=[Σw(|Fo2|-|Fc2|)2/Σw|Fo2|2]1/2.

Diffraction data ofcomplex 1 was got on Bruker AXS SMART APEX diffractometer,using Mo Kαradiation(λ=0.71073)with a CCD area detector.All the data were collected at 298 K and the structure was solved by direct methods,then subsequently refined on F2by using full-matrix least-squares techniques(SHELXL)[15],SADABS[16]absorption corrections were applied to the data.The calculation was performed using the Brucker Smart program.The details of the crystallographic data are shown in Table 1,and selected bond distances and angles are listed in Table 2.