《Table 3 H-bonding, C-H…πandπ…πinteractions parameters for 1》
本系列图表出处文件名:随高清版一同展现
《"基于4-甲基-3-苯基-5-(2-吡啶基)-1,2,4-三唑的Cu(Ⅱ)、Ni(Ⅱ)和Cd(Ⅱ)配合物的合成、晶体结构及性质(英文)"》
Symmetry codes:i-x+5/4,-y+1/4,z;ii1/2+x,1/4-y,7/4-z;iiix,-1+y,z;ivx,7/4-y,7/4-z;v3/4-x,y,7/4-z;vi3/2-x,-y,3/2-z;vii7/4-x,y,7/4-z;viii1/2-x,-y,3/2-z;Cg3:N1,N2,C2,N3,C1;Cg4:N4,C3,C4,C5,C6,C7;Cg5:C8,C9,C10,C11,C12,C13.
The picked single crystals were placed on a Bruker Smart APEXⅡCCD X-ray single crystal diffractometer(λ=0.071 073 nm),and the data were collected at 296(2)K.The crystal structures were solved by direct methods and refined on F2by fullmatrix least squares procedures using SHELXTL software[29].All non-hydrogen atoms were refined anisotropically,and all hydrogen atoms on carbon atoms were allowed to ride on the parent atoms geometrically.The hydrogen atoms of water molecules were found from the Fourier map,but not refined anisotropically.Crystallographic data of complexes 1~4 are shown in Table 1,selected bond lengths and bond angles for 1~4 are shown in Table 2,and H-bonding and C-H…πinteractions for 1~4 are shown in Table 3~6,respectively.
图表编号 | XD0043293200 严禁用于非法目的 |
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绘制时间 | 2019.01.10 |
作者 | 何卫卫、冯肆洋、瞿志荣、唐辉、王作祥 |
绘制单位 | 杭州师范大学有机硅化学及材料技术教育部重点实验室、杭州师范大学有机硅化学及材料技术教育部重点实验室、杭州师范大学有机硅化学及材料技术教育部重点实验室、东南大学化学化工学院、东南大学化学化工学院 |
更多格式 | 高清、无水印(增值服务) |