《Table 3 Results of accuracy and precision of the developed RP-HPLC method using MAC and its associa

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《指示稳定性的高效液相色谱方法和强制降解研究片剂型马西替坦中的杂质（英文）》

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Accuracy o f the develo ped m etho d is determ ined by m easuring the am o unt o f reco vered sam ples by injecting o r spiking kno w n co ncentratio ns o f im purities in the pure drug sam ple.The co ncentratio ns cho sen fo r accuracy determ inatio n w ere LOQ，100%，and 150%，specificatio n lim it as 0.5%（m ass percentage），w ith three replicate m easurem ents.The chro m ato gram s fo r the spiked sam ples fo r accuracy determ inatio n w ere sho w n in Fig.8 and the results are sum m arized in Table3.Results sho w ed that the develo ped m etho d can successfully reco ver the injected im purities w ithin the range o f 85%-115%，w hich is m o re accurate than o ther repo rted m etho do lo gies[33，34].