《Table 2Accuracy and precision results for five analytes in microdilysates at concentrations of LLOQ

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《Comparative brain pharmacokinetic study of Jiaotai Pills in normal and insomnic rats using brain microdialysis combinated with LC–MS/MS》

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The precision and accuracy data corresponding to LLOQ was shown in Table 2.The microdilysates concentration of five analytes is all 0.05 ng/m L.Table 3 summarized the intra-day and interday precisions and accuracies of five protoberberine-type alkaloids at three concentration levels.The accuracies ranged from-2.09%to 13.21%and the RSD was lower than 12.04%，which were well within the acceptance criteria of bioanalysis and indicated that the method was accurate，reliable，and reproducible.