《Table 1.Selected Bond Lengths () and Bond Angles (o) for 1》

《Table 1.Selected Bond Lengths () and Bond Angles (o) for 1》   提示：宽带有限、当前游客访问压缩模式
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《"Hydrothermal Synthesis, Crystal Structure and Luminescence Property of a 2D Manganese(Ⅱ) Coordination Polymer"》


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Symmetry codes:A-x，-y+1，-z+1；B x-1，y，z+1；C-x，-y+1，-z；D-x-1，-y+1，-z+1

Single crystal of 1 was obtained directly from the above preparation.All measurements were made on a Bruker Smart Apex-II CCD area detector by using graphite-monochromatic Mo K?（?=0.071073 nm）.Its crystal was mounted on a glass fiber at 296 K.The structure was solved by direct methods with SHELXS-97 program and refined by SHELXL-97[25]using full-matrix least-squares techniques on F2.All non-hydrogen atoms except the guest molecules were refined by full-matrix least-squares techniques with anisotropicdisplacementparametersandthe hydrogen atoms were geometrically fixed at the calculated positions attached to their parent atoms，and treated as riding atoms.Crystal data for 1，triclinic system，space group P1 with a=10.023（2），b=12.505（3），c=17.220（3）?，V=1934.4（8）?3，Z=1，C76H64Cl6Mn5N12O16，Mr=1888.79，Dc=1.621g/cm3，F（000）=959，GOOF=1.026，the final R=0.0276，w R=0.0727（w=1/[σ2 （Fo2）+（0.1071P）2]，where P=（Fo2+2Fc2）/3） ，（Δ/σ） max=0.001，（Δρ） max=0.445 and（Δρ）min=–0.384 e/?3.The selected bond lengths and bond angles and the hydrogen bond information for 1 are given in Tables 1 and 2，respectively.

图表编号XD0034856000    严禁用于非法目的
绘制时间2019.01.01
作者郁有祝、常颂扬、韩曦、陈广鑫、轩亚威、武现丽、王芳
绘制单位College of Chemistry and Environmental Engineering,Anyang Institute of Technology、College of Chemistry and Environmental Engineering,Anyang Institute of Technology、College of Chemistry and Environmental Engineering,Anyang Institute of Technology、College o
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