《Table 2.Selected Bond Lengths () and Bond Angles (°) for Compound 2》

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《"Three Two-dimensional Heterometallic Chalcogenides[TM(tren)][InSbSe_3S](TM = Fe, Co, Mn): Syntheses,Crystal Structures, and Properties"》

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Symmetry transformations used to generate the equivalent atoms:#1:x，–y+1/2，z–1/2；#2:–x+2，–y，–z；#3:x，–y+1/2，z+1/2

Suitable crystals were put on a Bruker Apex II CCD diffractometer and equipped with graphitemonochromatized Mo Kαradiation（?=0.71073?）at room temperature.The dimensions of the block orange crystal 1 are 0.28?0.25?0.21 mm3.A total of 7103 reflections were collected，of which 2769（Rint=0.0760）independent reflections in the range of2.43o≤θ≤25.00owith–13≤h≤12，–11≤k≤16and–13≤l≤12 were collected at 296（2）K.The dimensions of the block-shaped dark green crystal 2are 0.25?0.21?0.15 mm3.A total of 7883reflections were collected，and among them 2867（Rint=0.0640）independent reflections in the range of1.92o≤θ≤25.00owith–14≤h≤13，–16≤k≤11and–13≤l≤13 were collected at 296（2）K.A total of 8074 reflections for 3（0.25?0.21?0.15 mm3）were collected，of which 2966（Rint=0.1021）independent reflections in the range of 1.90o≤θ≤25.00owith–14≤h≤14，–16≤k≤16，–13≤l≤9were collected at 296（2）K.The structures were solved by direct methods using SHELXS-97，and refined against F2 using SHELXL-97[25].The selected bond lengths and bond angles for 1，2 and 3are given in Tables 1，2 and 3，respectively.