《Table 2.Selected Bond Lengths () and Bond Angles (°) for 1 and 2》
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《"Flexible Bis(benzimidazole)-based Ligands Directed the Structure Characteristics of Coordination Polymers Based on Diphenic Acid Co-ligands:Syntheses, Structures and Properties"》
Symmetry transformations used to generate equivalent atoms for 1:#1:x+1/2，–y+3/2，–z+1；#2:x–1/2，–y+5/2，–z+1；#3:x–1/2，–y+3/2，–z+1；#4:x+1/2，–y+5/2，–z+1Symmetry transformations used to generate equivalent atoms for 2:#1:–x+1/2，–y+1/2，–z+
The well-shaped single crystals of complexes 1and 2 were selected for X-ray diffraction study.The unit cell parameters and intensity data were collected at 293 K on a Bruker SMART APEX II CCD diffractometer using a graphite-monochromated Mo Kα（λ=0.071073 nm）radiation.The structures were solved by direct methods using SHELXS program[20]package and refined by fullmatrix least-squares fitting on F2 by SHEXL-97[21].All non-hydrogen atoms were refined anisotropically.All hydrogen atoms of organic ligands were placed in geometrically idealized positions and constrained to ride on their parent atoms（Complex1:C–H=0.97?with Uiso （H）=1.2Ueq（C）for methylene groups，C–H=0.93?with Uiso（H）=1.4Ueq（C）for aromatic rings.Complex 2:C–H=0.97?with Uiso（H）=1.2Ueq（C）for methylene groups，C–H=0.93?with Uiso（H）=1.2Ueq（C）for aromatic rings） .The details of crystal parameters are summarized in Table 1，and the selected bond lengths are listed in Table 2.
| 图表编号 | XD0034856100 严禁用于非法目的 |
|---|---|
| 绘制时间 | 2019.01.01 |
| 作者 | 屠长征、杨玉亭、许丽丽、晏帮领、汪帆 |
| 绘制单位 | College of Chemistry and Environmental Science,Qujing Normal University、College of Chemistry and Environmental Science,Qujing Normal University、College of Chemistry and Environmental Science,Qujing Normal University、College of Chemistry and Environmental |
| 更多格式 | 高清、无水印（增值服务） |
