《Table 1.Physicochemical properties of C-SBA-15 and DBD-SBA-15.》

《Table 1.Physicochemical properties of C-SBA-15 and DBD-SBA-15.》   提示:宽带有限、当前游客访问压缩模式
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《Fast and low-temperature elimination of organic templates from SBA-15 using dielectric barrier discharge plasma》


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Figure 7 shows the thermo gravimetric(TG)analysis results of all samples in the temperature range from 150°C to 800°C.It should be noted that the weight losses below 200°C,assigned mainly to the physically adsorbed and chemically adsorbed water,were nearly the same for C-SBA-15 and DBD-SBA-15. The weight loss about 200°C would be attributed mainly to the dehydroxylation by condensation of silanol groups[23].The weight losses corresponding to the as-synthesized,plasma treated and calcinations treated SBA-15 were 39.3%,8.3%and5.5%,respectively.Therefore,the DBD plasma method can efficiently remove the template at a relatively low temperature,which will abundantly preserve the Si–OH groups and avoid the shrinkage of the frame structure of SBA-15.Further studies on the impact of particle size on the performance of the DBD treatment are currently underway in our laboratory.