《Analytical Chemistry of Ruthenium》
| 作者 | 编者 |
|---|---|
| 出版 | Ann Arbor-Humphrey Science Publishers |
| 参考页数 | 250 |
| 出版时间 | 1963（求助前请核对） 目录预览 |
| ISBN号 | 无 — 求助条款 |
| PDF编号 | 812506348（仅供预览，未存储实际文件） |
| 求助格式 | 扫描PDF（若分多册发行，每次仅能受理1册） |
Chapter Ⅰ：PHYSICOCHEMICAL AND ANALYTICAL CHARACTERISTICS OF RUTHENIUM AND ITS COMPOUNDS1
Chapter Ⅱ：DETECTION OF RUTHENIUM12
Inorganic reagents for ruthenium12
Organic reagents for ruthenium16
Spot tests for ruthenium27
Chemical microscopic detection of ruthenium30
Detection of ruthenium by the catalytic action of its compounds35
Detection of ruthenium in a mixture of cations35
Chapter Ⅲ：CHEMICAL AND INSTRUMENTAL METHODS FOR THE DETERMINATION OF RUTHENIUM37
Gravimetric methods of determination of ruthenium37
Volumetric methods of determination of ruthenium52
Potentiometric titration methods57
Photometric determinations of ruthenium60
Fluorescence method of determination of ruthenium by 5-methyl-1，10-phenanthroline99
Electrochemical methods100
Polarographic methods117
Spectroscopic and X-ray methods127
Radiochemical methods132
Chapter Ⅳ：SEPARATION OF RUTHENIUM FROM THE ACCOMPANYING ELEMENTS144
Methods involving isolation of ruthenium tetroxide144
Separation of osmium and ruthenium tetroxides163
Separation of ruthenium from platinum metals166
Separation of ruthenium from alkaline earth metals and magnesium168
Chromatographic separation of ruthenium from other elements169
Chapter Ⅴ：DETERMINATION OF RUTHENIUM IN NATURAL MATERIALS AND INDUSTRIAL PRODUCTS174
The separation of platinum metals from the accompanying elements175
Assay methods for the separation of platinum metals176
Chemical methods of separation of platinum metals181
Determination of ruthenium in concentrates190
Determination of ruthenium in slurries and slags192
Determination of ruthenium in osmiridium194
Determination of ruthenium in the wastes of refining industry196
Analysis of silver bead197
Analysis of alloys containing ruthenium198
Determination of impurities in refined ruthenium202
Analytical procedures for the determination of ruthenium in various materials203
APPENDIX214
Determination of ruthenium in fluorides214
Methods of preparation of various ruthenium compounds216
Ruthenium compounds used as indicators220
BIBLIOGRAPHY223
SUBJECT INDEX247
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