《Table 1 Case studies of fluid inclusions within low-T halite》

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《Fluid Inclusions in Surface-temperature Halite: Sample Preparation and Application》

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Measurements of homogenization temperature of fluid inclusions within low-temperature halite often involves freezing halite samples for 3 days to 4 weeks at-10–-20℃（Table 1）.Although the cooling-nucleation method was widely used，the most appropriate cooling time and conditions have not been documented.In this study，halite cleavage fragments of laboratory-grown crystals were cooled in the heating/freezing stage for 40–50 minutes at-18℃，or frozen in a freezer for 1，10，20 and 40 days，respectively，at-18℃.The homogenization temperatures of fluid inclusions in halite samples prepared with these two methods were then measured and compared，to determine the optimum cooling-nucleation procedure for halite samples.