《HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY ADVANCES AND PERSPECTIVES VOLUME 2》求取 ⇩

LIST OF CONTRIBUTORS7

CONSPECTUS9

PREFACE11

CONTENTS OF VOLUME 113

Optimization in Liquid Chromatography Georges Guiochon1

Ⅰ．Introduction1

Ⅱ．Resolution and Efficiency2

Ⅲ．AnalysiS Time,Flowrate, and Pressure6

Ⅳ．Flow Velocity and Column Efficiency7

Ⅴ．What to Optimize in Liquid Chromatography15

Ⅵ．Equations Used for Optimization17

Ⅶ．WayS to Achieve 5000 Plates in 5 Minutes19

Ⅷ．Column Performance at Minimum Inlet Pressure29

Ⅸ．Critical Minimum Pressure33

Ⅹ．Achievement of Fastest Analyses35

Ⅺ．Practical Considerations39

Ⅻ．Equipment Specifications43

ⅩⅢ．Conclusions52

References54

Liquid Chromatography on Silica and Alumina as Stationary Phases Heinz Engelhardt and Helmut ElgassⅠ．Introduction57

Ⅱ．Stationary Phases60

Ⅲ．Role of the Eluent70

Ⅳ．Effect of Sample Structure on Retention90

Ⅴ．Anisocratic Analysis92

Ⅵ Theory of Adsorption Chromatography101

Ⅶ．Selected Applications104

Ⅷ．Prospects106

References108

Reversed-Phase Chromatography Wayne R．Melander and Csaba HorváthⅠ．Introduction114

Ⅱ．The Stationary Phase123

Ⅲ．The Mobile Phase165

Ⅳ．Effect of Temperature192

Ⅴ．Theory of Reversed-Phase Chromatography201

Ⅵ．Modulation of Selectivity by Secondary Equilibria229

Ⅶ．Physicochemical Measurements266

Ⅷ．Selected Analytical Applications279

Notation299

References303

Index321

Erratum341