《Table 3 Selected bond angles for 1 and 2》

《Table 3 Selected bond angles for 1 and 2》   提示:宽带有限、当前游客访问压缩模式
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《"Syntheses, Crystal Structures, and Fluorescence Properties of Two 2D→2D Coordination Polymers Based on the Flexible 4-Substituted Bis(1,2,4-triazole) Ligand"》


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Symmetry codes:#1-1/2+x,1/2-y,+z for 1;-1/2+x,1/2-y,-1/2+z for 2

The diffraction data of 1 and 2 were collected on the Rigaku Saturn 724 CCD diffractometer with graphite monochromated MoKa radiation(λ=0.071 075 nm)at293.15 K.The intensities were collected byω-scan and reduced on the CrystalClear(Rigaku Inc.,2007),and a multi-scan absorption correction was applied.All nonhydrogen atoms were refined anisotropically on F2 by full-matrix least-squares techniques using SHELXL crystallographic package[24,25].All the hydrogen atoms were determined with theoretical calculations and refined isotropically.The parameters of the crystal data collection and refinement of 1 and 2 are given in Table 1.The selected bond lengths and bond angles of 1 and 2 are listed in Tables 2 and 3.