《Table 1 Growth process parameters and as-growth crystal type at different P2O5 contents》

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《三元磷酸氧碲晶体的生长（英文）》

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Figure 2 shows the XRPD patterns of the three as-grown crystals.Clearly，the crystals are Te8P4O26，Te3P2O11，and Te2P2O9.The XRPD patterns are in reasonable agreement with the standard data，and no impurity peaks appear.All the diffraction peaks of the as-grown crystals are sharp in the measured 2θrange，indicating that the three crystals are well-crystallized[14].The crystal types correspond to the six different types of raw materials see Table 1.